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A simplified FIR chemometric method for simultaneous determination of four oxidation parameters of frying canola oil
(PERGAMON-ELSEVIER SCIENCE LTD, 2015) Talpur, M. Younis; Hassan, S. Sara; Sherazi, S. T. H.; Mahesar, S. A.; Kara, Huseyin; Kandhro, Aftab A.; Sirajuddin
Transmission Fourier transform infrared (FTIR) spectroscopic method using 100 mu m KCl cell was applied for the determination of total polar compounds (TPC), carbonyl value (CV), conjugated diene (CD) and conjugated triene (CT) in canola oil (CLO) during potato chips frying at 180 degrees C. The calibration models were developed for TPC, CV, CD and CT using partial least square (PLS) chemometric technique. Excellent regression coefficients (R-2) and root mean square error of prediction values for TPC, CV, CD and CT were found to be 0.999, 0.992, 0.998 and 0.999 and 0.809, 0.690, 1.26 and 0.735, respectively. The developed calibration models were applied on samples of canola oil drawn during potato chips frying process. A linear relationship was obtained between CD and TPC with a good correlation of coefficient (R-2 = 0.9816). Results of the study clearly indicated that transmission FTIR-PLS method could be used for quick and precise evaluation of oxidative changes during the frying process without using any organic solvent. (C) 2015 Elsevier B.V. All rights reserved.