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Rapid Determination of Free Fatty Acid Content in Waste Deodorizer Distillates Using Single Bounce-Attenuated Total Reflectance-FTIR Spectroscopy
(AOAC INT, 2012) Naz, Saba; Tufail, Saved; Sherazi, Hussain; Talpur, Farah N.; Mahesar, Sarfaraz A.; Kara, Huseyin
A simple, rapid, economical, and environmentally friendly analytical method was developed for the quantitative assessment of free fatty acids (FFAs) present in deodorizer distillates and crude oils by single bounce-attenuated total reflectance-FTIR spectroscopy. Partial least squares was applied for the calibration model based on the peak region of the carbonyl group (C=0) from 1726 to 1664 cm(-1) associated with the FFAs. The proposed method totally avoided the use of organic solvents or costly standards and could be applied easily in the oil processing industry. The accuracy of the method was checked by comparison to a conventional standard American Oil Chemists' Society (AOCS) titrimetric procedure, which provided good correlation (R = 0.99980), with an SD of 0.05%. Therefore, the proposed method could be used as an alternate to the AOCS titrimetric method for the quantitative determination of FFAs especially in deodorizer distillates.