Synthesis and Evaluation of Chromate and Arsenate Anions Extraction Ability of a N-methylglucamine Derivative of Calix[4]arene Immobilized Onto Magnetic Nanoparticles

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dc.contributor.authorSayın, Serkan
dc.contributor.authorÖzcan, Fatih
dc.contributor.authorYılmaz, Mustafa
dc.date.accessioned2020-03-26T18:05:05Z
dc.date.available2020-03-26T18:05:05Z
dc.date.issued2010
dc.departmentSelçuk Üniversitesien_US
dc.description.abstractIn this study, 5,17-bis-[(N-methylglucamine)methyl]-25,26,27,28-tetrahydroxy-calix[4]arene (3) was synthesized by the treatment of calix[4]arene with a secondary amine N-methylglucamine and formaldehyde. The calixarene derivative (3) was characterized by a combination of FTIR, H-1 NMR and elemental analyses. Followingly, using the macrocyclic building block, the compound 3 was immobilized by [3-(2,3-epoxypropoxy)propyl]trimethoxysilane-modified Fe3O4 magnetite nanoparticles (EPPTMS-MN). The prepared calix[4]arene immobilized material was characterized by a combination of Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM) and thermogravimetric analyses (TGA). Moreover, the studies regarding the removal of arsenate and dichromate ions from the aqueous solutions were also carried out by using the compound in solid-liquid extraction experiments. It was found that the calix[4]arene-based magnetic material has high extraction ability towards dichromate and arsenate anions in 66% (at pH 1.5) and in 86% (at pH 3.5), respectively.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK)Turkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [107T873]; Research Foundation of Selcuk University (BAP)Selcuk Universityen_US
dc.description.sponsorshipWe would like to thank the Scientific and Technological Research Council of Turkey (TUBITAK Grant no. 107T873) and the Research Foundation of Selcuk University (BAP) for financial support of this work.en_US
dc.identifier.citationSayın, S., Özcan, F., Yilmaz, M., (2010). Synthesis and Evaluation of Chromate and Arsenate Anions Extraction Ability of a N-methylglucamine Derivative of Calix[4]arene Immobilized Onto Magnetic Nanoparticles. Journal of Hazardous Materials, 178(2010), 312-319. Doi:10.1016/j.jhazmat.2010.01.080
dc.identifier.doi10.1016/j.jhazmat.2010.01.080en_US
dc.identifier.endpage319en_US
dc.identifier.issn0304-3894en_US
dc.identifier.issn1873-3336en_US
dc.identifier.issue01.03.2020en_US
dc.identifier.pmid20133056en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage312en_US
dc.identifier.urihttps://dx.doi.org/10.1016/j.jhazmat.2010.01.080
dc.identifier.urihttps://hdl.handle.net/20.500.12395/25301
dc.identifier.volume178en_US
dc.identifier.wosWOS:000278056300041en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.institutionauthorSayın, Serkan
dc.institutionauthorÖzcan, Fatih
dc.institutionauthorYılmaz, Mustafa
dc.language.isoenen_US
dc.publisherELSEVIER SCIENCE BVen_US
dc.relation.ispartofJournal of Hazardous Materialsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.selcuk20240510_oaigen_US
dc.subjectCalix[4]areneen_US
dc.subjectDichromate anionen_US
dc.subjectArsenate anionen_US
dc.subjectSorptionen_US
dc.subjectMagnetic nanoparticlesen_US
dc.titleSynthesis and Evaluation of Chromate and Arsenate Anions Extraction Ability of a N-methylglucamine Derivative of Calix[4]arene Immobilized Onto Magnetic Nanoparticlesen_US
dc.typeArticleen_US

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